HOW TO SUBMIT SAMPLES

For the analysis of your sample(s), you may send  them  by post along with a covering letter from the Head / Guide,  on your College/Institute Original Letter Head, demand draft and requisition form for the use of respective instrument. The   letter should be addressed to The Head, SAIF, IIT Patna. You can also submit samples directly in person. Please contact  SO SAIF  before visiting SAIF IIT Patna so that  you can save your time.

Address for sending the samples

          Head, Sophisticated Analytical Instrument Facility,
          Science Block -04, Ground floor, Room no. 11,
          Indian Institute of Technology Patna
          Bihta Campus, Amhara Road, Bihta, District - Patna
          Bihar, INDIA, PIN - 801106
          Phone No: 06115-233-686 
          E-mail: This email address is being protected from spambots. You need JavaScript enabled to view it.

-       Your slot for respective sample analysis will be confirmed through email.
-       If Samples are received without covering letter/DD, the samples will not be analysed.Separate sample should be sent for different analysis.
-       Interpretation of spectra/data is not undertaken normally. In special cases this service can be provided on payment on extra charges.
-       As soon as the analysis is over, the spectra/data along with the receipt / bill will be sent to the users.
-       If you want samples back please mention in your letter.
        Kindly collect your samples back at the time of collecting your data. Samples which are not collected within a week from the date of data collected /sample analysis will be disposed of immediately without any further notice.

Note

As per the guidelines of the Department of Science and Technology (DST), in all publications of research work,  where in the  analytical services of the SAIF have been made use of,  the DST and the SAIF, IIT Patna shall be duly acknowledged.  Kindly send us the publication reference (Journal name/volume number/names of the authors/date of issue of the publication etc) to us.

A list of charges for measurements, as fixed by the Department of Science & Technology, New Delhi, is taken. Please note that:

  • The charges mentioned for analysis of samples are received from users within India only.
  • For abroad users, please contact SAIF by Email directly.
  • Charges are subject to change periodically.

Kindly add GST 18% on Instrument Charges in accordance with Government of India instructions.

CRYSTALLOGRAPHY

S. No.

Facility

Parameter

Charges(Rs.) without Tax

Industries

R&D and National Labs

Academic and Educational Institutions

Internal user

1

Single crystal X-Ray Diffractometer (SC-XRD)

For structure determination, charges are extra. (Pl. contact the operator)

Cell Parameters

Rs.2500 /- per Measurement

Rs.1500/- per Measurement

Rs.500/- per Measurement

Rs. 250/- per Measurement

Data Collection

Rs.11000/- per Measurement

Rs.6600/- per Measurement

Rs.2200/- per Measurement

Rs.1100/- per Measurement

Data Structure*

Rs. 20000/- per Measurement

Rs. 12000/- per Measurement

Rs.4000/- per Measurement

Rs.2000/- per Measurement

Data at low temperature

Rs.20000/- per Measurement

Rs.12000/- per Measurement

Rs.4000/- per Measurement

Rs.2000/- per Measurement

Data & structure at low temperature

Rs. 28000/- per Measurement

Rs. 16800/- per Measurement

Rs. 5600/- per Measurement

Rs.2800/- per Measurement

High Resolution - Liquid Chromatography Mass Spectrometry (HR-LCMS)

S. No.

Facility

Charges(Rs.) without Tax

Industries

R&D and National Labs

Academic and Educational Institutions

Internal user

2.

Mass -Direct infusion

(HRMS)

Rs.3500/- per sample

Rs.2100/- per sample

Rs.700/- per sample

Rs.350/- per sample

MS-MS

Rs.5000/- per sample

Rs.3000/- per sample

Rs.1000/- per sample

Rs.500/- per sample

HR-LCMS

Rs.5500/- per sample

Rs.3300/- per sample

Rs.1100/- per sample

Rs.550/- per sample

                     

 

Bulk measurement – Type 1

S. No.

Facility

Parameter

Charges(Rs.) without Tax for 10 measurements

Industries

R&D and National Labs

Academic and Educational Institutions

Internal user

1.

Single crystal X-Ray Diffractometer (SC-XRD)

Data Collection
at  room temperature

Rs.80,000/-

Rs.48000/-

Rs.16000/-

Rs.8000 /-

 

High Resolution - Liquid Chromatography Mass Spectrometry (HR-LCMS)

S. No.

Facility

Charges(Rs.) without Tax for 10 samples

Industries

R&D and National Labs

Academic and Educational Institutions

Internal user

2.

 (HRMS)

Rs.25000 /-

Rs.15000 /-

Rs.5000 /-

Rs.2500 /-



Bulk measurement – Type 2

S. No.

Facility

Parameter

Charges(Rs.) without Tax for 400 hours

Industries

R&D and National Labs

Academic and Educational Institutions

Internal user

 1.

Single crystal X-Ray Diffractometer (SC-XRD)

Data Collection
at  room temperature

Rs. 2,00,000/-

Rs. 1,20,000/-

Rs.40,000/-

Rs.20,000 /-

 

High Resolution - Liquid Chromatography Mass Spectrometry (HR-LCMS)

S. No.

Facility

Charges(Rs.) without Tax for 100 samples/20 hours

Industries

R&D and National Labs

Academic and Educational Institutions

Internal user

2.

 (HRMS)

Rs. 2,00,000/-

Rs. 1,20,000/-

Rs.40,000/-

Rs.20,000 /-

 

Terms and conditions for the bulk measurements Type 2:

  1. Bulk measurements can be booked either in institute/department level or individual user level.
  2. The user side will provide fellow/manpower equivalent to a researcher (minimum qualification needed is M.Sc or B.Tech) who will assist Scientific Officer, SAIF, IITP (or responsible SAIF, IITP personal) during the measurements. For one bulk booking only one person will be allowed for assistance.
  3. SAIF, IITP will provide the researchers necessary training without any additional cost beforehand (at least for 2 -3 days).
  4. SAIF, IITP will not responsible for travel and accommodation of the researcher. SAIF, IITP also not provide any additional fellowship or similar announces for such assistance.
  5. The outside users may avail IITP guesthouse facility (depends on the availability) on self-finance with the approval of competent authority.
  6. The booking will be valid for 12 months. (Will be extended in case the machine is not available or not in working condition within the timeframe).
  7. The user can do all samples at one time or at different time intervals. The time will be allotted to the users as per the availability.

Data Structure*
"These are the minimum charges. Additional charges may be levied depending on the nature and complexity of the problem.

 

500 MHz NMR Spectrometer

Liquid Probe

Experiment (S)

Solvent

Quantity Of sample

 

 

No. of Scans

Charges (In Rs.) for

Industries

 

Charges (In Rs.) for

R&D and National Labs

Charges (In Rs.) for

Academic and Educational Institutions

Charges (In Rs.) for

Internal user

1H, 19F &31P NMR

 

 

 

CDCl3

 

35 mg

16

900

540

180

90

<3 mg

32

1150

690

230

115

1 mg

128

1700

1020

340

170

DMSO-D6

 

35 mg

16

1350

810

270

135

<3 mg

32

1600

960

320

160

1 mg

128

2200

1320

440

220

D2O

 

35 mg

16

900

540

180

90

<3 mg

32

1150

690

230

115

1 mg

128

1700

1020

340

170

Benzene -D6

 

35 mg

16

1600

960

320

160

<3 mg

32

1800

1080

360

180

1 mg

128

2500

1500

500

250

13C NMR/DEPT

 

 

 

CDCl3

 

>25 mg

256

1900

1140

380

190

<25 mg

512

2250

1350

450

225

1015 mg

1024

3100

1860

620

310

DMSO-D6

 

>25 mg

256

2250

1350

450

225

<25 mg

512

2650

1590

530

265

1015 mg

1024

3550

2130

710

355

D2O

 

>25 mg

256

1900

1140

380

190

<25 mg

512

2250

1350

450

225

1015 mg

1024

3100

1860

620

310

Benzene -D6

 

>25 mg

256

2600

1560

520

260

<25 mg

512

3050

1830

610

305

1015 mg

1024

3850

2310

770

385

 

2D/COSY/NOESY/ DOSY/ HSQC/HMQC/HMBC/TOCSY

 

 

CDCl3

 

>15 mg

128

1700

1020

340

170

512

2650

1590

530

265

1024

3350

2010

670

335

DMSO-D6

 

>15 mg

128

2250

1350

450

225

512

3100

1860

620

310

1024

3750

2250

750

375

D2O

 

>15 mg

128

1700

1020

340

170

512

2650

1590

530

265

1024

3350

2010

670

335

Benzene -D6

 

>15 mg

128

2450

1470

490

245

512

3400

2040

680

340

1024

4000

2400

800

400

Solid Probe

31P/13C/DEPT

Quantity Of sample

 

 

100 mg

 

No. of Scans

Charges (In Rs.) for

Industries

 

Charges (In Rs.) for

R&D and National Labs

Charges (In Rs.) for

Academic and Educational Institutions

Charges (In Rs.) for

Internal user

 

256

10500

6300

2100

1050

512

12000

7200

2400

1200

1024

15000

9000

3000

1500

Hourly Basis Charges

Liquid Probe

Charges (In Rs.) for

Industries

 

Charges (In Rs.) for

R&D and National Labs

Charges (In Rs.) for

Academic and Educational Institutions

Charges (In Rs.) for

Internal user

 

4000 per hour

2400 per hour

800 per hour

400 per hour

Solid Probe

Charges (In Rs.) for

Industries

 

Charges (In Rs.) for

R&D and National Labs

Charges (In Rs.) for

Academic and Educational Institutions

Charges (In Rs.) for

Internal user

 

14000 per hour

8400 per hour

2800 per hour

1400 per hour

Note: In case of hourly basis, user has to provide deuterated solvents for liquid probe.

  • For solid probe data collection side band separation required or not required please mention. If required extra @2%  charges will be required.
  • IIT, Patna has variable temperature data collection setup in both liquid and solid probes. An extra@10 charges will be applicable for using VT data.
  • In liquid state the data can be collected from  -90º C to +130ºC range. In solid state the data can be collected from 25ºC to 50ºC range with maximum rotation speed 10k.
  • Other than the above mention solvent the user has to supply the deuterared NMR solvents and charges using CDCl3 will be applicable in that case.
  • Charges mentioned here are excluding GST. Please add 18 % GST along with the charges as per Government Regulation.
  • If the time exceeds for the specialized experiment as per user instruction, every additional experiment/time (30 min. additional time) will be charged thereof with Rs. 500/-or academic institutes, Rs. 1500/- for R&D and National Labs and Rs. 2500/- for Industries.

* Note: Additional Rs 100/- towards postal charge if results are to be posted.

Mode of Payment

Payments are to be made only by crossed demand draft (DD).

The Demand Draft should be in favour of

"The Registrar, IIT Patna"

Letter, DD & Samples send to

Head, SAIF,
Science Block -04, Ground floor, Room no. 11, 
IIT Patna Bihta Campus, Amhara Road,
Bihta, District – Patna.
Bihar, INDIA, PIN – 801106
--------------------------------------------------

* Note: To know about the status of the sample, please contact at saif_office[at]iitp.ac.in, vc[at]iitp.ac.in